Table 1.

Data collection and refinement statistics

GFLD·Cu
Data collection
    Space groupP212121
    Cell dimensions
        a, b, c (Å)34.05, 49.07, 66.16
    Resolution (Å)a30.28–1.75 (1.81–1.75)
    Rsym6.3 (42.9)
    I/σI12.99 (3.19)
    Completeness (%)99.85 (100.00)
    Redundancy5.9 (6.0)
Refinement
    Resolution (Å)30.28–1.75 (1.81–1.75)
    n reflections11674
    Rwork/Rfree0.1807/0.2303
    n atoms
        Protein/ligand/water826/7/52
    B-factors
        Protein/ligand/water44.8/52.8/53.9
    rms deviations
        Bond lengths (Å)0.007
        Bond angles (°)1.16

  • Values in parentheses are for the highest resolution shell.

  • ↵aData measured on one crystal.